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Beilstein J. Org. Chem. 2018, 14, 2384–2393, doi:10.3762/bjoc.14.214
Graphical Abstract
Figure 1: Structures of stereoisomers of 3,4,5-tris(2-methoxyphenyl)-2,6-dimethylpyridines determined by X-ra...
Figure 2: Graphical representation of kinetic, time-dependent 1H NMR analysis of (syn)-7 (100 °C).
Figure 3: Graphical representation of kinetic, time-dependent 1H NMR analysis of (syn)-10 (120 °C).
Figure 4: HT-NMR (300 MHz, DMSO-d6) spectra of A) (syn)-7. B) (syn)-10. Only the upfield (ca. 3.4–4 ppm) regi...
Figure 5: Summary of the results for coupling with ortho-substituted phenylboronic acid for triaryl products.
Figure 6: Summary of results for coupling with ortho-substituted phenylboronic acid for diaryl products.
Figure 7: Proposed intermediates for the 1,2-addition of 5 with methoxy group. A) Oxidative addition step. B)...
Figure 8: Proposed intermediates for the 1,3-addition with methoxy group. A) Oxidative addition step. B) Tran...
Figure 9: Proposed intermediates for the 1,2-addition with chlorine atom. A) Oxidative addition step. B) Tran...
Figure 10: Proposed intermediates for the 1,3-addition with chlorine atom. A) Oxidative addition step. B) Tran...